Health preserving medicinal liquor and brewing method thereof
1. The health-preserving medicinal liquor is characterized by comprising the following components in parts by weight:
1 part of oyster, 1 part of spina date seed, 3 parts of medlar, 3 parts of ginseng, 4 parts of Chinese date, 2 parts of rhizoma polygonati, 3 parts of propolis, 3 parts of cervus elaphus linnaeus, 2 parts of gecko, 3 parts of cervus elaphus linnaeus embryo, 3 parts of astragalus membranaceus, 2 parts of dendrobe, 2 parts of epimedium, 2 parts of semen cuscutae, 1 part of ginkgo leaf, 3 parts of honey, 1 part of semen coicis, 1 part of arillus longan, 2 parts of liquorice, 1 part of cinnamon, 2 parts of phaseolus calcaratus, 3 parts of endothelium corneum gigeriae galli, 2 parts of fructus alpiniae oxyphyllae, 1 part of honeysuckle and 3 parts of radix puerariae;
the medicinal liquor is prepared by the following steps:
the method comprises the following steps: mixing Concha Ostreae, propolis, cornu Cervi Pantotrichum, Gecko, embryo Cervi, Mel, and endothelium corneum Gigeriae Galli to obtain Chinese medicinal mixture A;
step two: mixing semen Ziziphi Spinosae, fructus Lycii, Ginseng radix, fructus Jujubae, rhizoma Polygonati, radix astragali, herba Dendrobii, herba Epimedii, semen Cuscutae, folium Ginkgo, Coicis semen, arillus longan, Glycyrrhrizae radix, cortex Cinnamomi, semen Phaseoli, fructus Alpinae Oxyphyllae, flos Lonicerae, and radix Puerariae to obtain Chinese medicinal mixture B;
step three: respectively adding hot water from a heat recovery chamber into the traditional Chinese medicine mixture A and the traditional Chinese medicine mixture B, soaking for 12h, taking out the traditional Chinese medicine mixture A, steaming for 60 min on strong fire, cooling for later use, taking out the traditional Chinese medicine mixture B, putting into a container, boiling for 30min on strong fire, and cooling for later use;
step four: adding 60-degree Chinese liquor into the steamed Chinese medicinal mixture A and the boiled Chinese medicinal mixture B respectively, and soaking for 15 days;
step five: putting the Chinese medicinal mixture A, the Chinese medicinal mixture B, the Chinese medicinal soaking solution, the water soaking solution and the wine grain after soaking in the white wine into a cellar pool for fermenting for 90 days to obtain a fermented material;
step six: adding the fermented material into a brewing distiller (102) of a medicated wine brewing device, spraying fire into an inner cavity of a combustion chamber (105) through a flame sprayer (106) to heat the brewing distiller (102), heating the brewing distiller (102) to distill the fermented material, enabling alcohol to form alcohol vapor to rise, entering a return pipe (107), liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller (102), and enabling the rest of the alcohol vapor to enter a heat recovery chamber (104) through a vapor guide pipe (108);
step seven: cooling clean water is injected into the heat recovery chamber from the water inlet pipe (117), alcohol steam is shunted through the shunt pipe (109) and enters the plurality of condensation pipes (110), drops are formed by cooling of the cooling clean water, medicinal liquor is obtained, the medicinal liquor is converged through the confluence pipe (111), enters the guide pipe (113), enters the discharging pipe (114) through flow guiding, a valve is opened, the medicinal liquor is discharged from the discharging pipe (114) and collected in the collection tank (116), and sealing is carried out.
2. The health preserving medicated wine as claimed in claim 1, wherein the medicated wine brewing device comprises a mounting base (101), a brewing distiller (102), a discharging box (103) and a heat recovery chamber (104), wherein the discharging box (103) is mounted on one side of the mounting base (101), the brewing distiller (102) is embedded and mounted on the mounting base (101), and the heat recovery chamber (104) is mounted at the top of the discharging box (103);
be provided with combustion chamber (105) in the inner chamber of installation base (101), flame thrower (106) is installed to the inner chamber bottom of combustion chamber (105), flame thrower (106) is located wine brewing distiller (102) under, the sealing door is installed in one side rotation of blow down case (103), be provided with aseptic room (115) in the inner chamber of blow down case (103), place in collecting tank (116) in the inner chamber of aseptic room (115), collecting tank (116) are located blow down pipe (114), install the valve on blow down pipe (114), blow down pipe (114) are installed on the bottom of honeycomb duct (113), blow down pipe (114) run through and are installed at the top of blow down case (103), return pipe (107) are installed at the top of wine brewing distiller (102), steam conduit (108) are installed on the top of return pipe (107), one end of the steam guide pipe (108) far away from the return pipe (107) runs through the top of the heat recovery chamber (104) and is connected to the top of the shunt pipe (109), a plurality of condensation pipes (110) are installed at the bottom of the shunt pipe (109) in an equal distance mode, the condensation pipes (110) are S-shaped, the bottom ends of the condensation pipes (110) are communicated to the top of the collecting pipe (111), the two ends of the shunt pipe (109) and the collecting pipe (111) are installed on the two sides of the inner wall of the heat recovery chamber (104) respectively, the bottom of the collecting pipe (111) is provided with a flow guide hopper (112), and the bottom end of the flow guide hopper (112) is communicated to the top end of the flow guide pipe (113).
3. The health preserving medicated wine as claimed in claim 2, wherein a water inlet pipe (117) is installed at the top of one end of the heat recovery chamber (104), a water drain pipe (118) and an air release pipe (119) are installed at the bottom of one side of the heat recovery chamber (104), the air release pipe (119) is installed at one end of the flow guide hopper (112), and the air release pipe (119) is arc-shaped with an upward port.
4. The health preserving medicinal liquor as claimed in claim 2, wherein the heat recovery chamber (104) is formed by splicing a plurality of composite plates, each composite plate comprises a first stainless steel layer (120), a heat insulating layer (121) and a second stainless steel layer (122), the heat insulating layer (121) is positioned between the first stainless steel layer (120) and the second stainless steel layer (122), and the heat insulating layer (121) is fixedly connected with the first stainless steel layer (120) and the second stainless steel layer (122).
5. The health preserving medicinal liquor as claimed in claim 4, wherein the preparation method of the heat preserving and insulating layer (121) is as follows
A1: weighing 100-200 parts of heat-insulating resin, 3.5-7.0 parts of surfactant, 6-12 parts of foaming agent and 15-21 parts of curing agent according to parts by weight for later use;
a2: adding the heat-preservation and heat-insulation resin and the surfactant into a high-speed dispersing machine, and uniformly mixing to obtain a mixture A;
a3: adding a foaming agent into the mixture A for continuous dispersion, and uniformly mixing to obtain a mixture B;
a4: and adding the curing agent into the mixture B for continuous dispersion, uniformly mixing, pouring into a preheated mold, placing the mold in a constant-temperature oven at the temperature of 75-80 ℃ for drying for 10-20min, taking out the mold, and curing at the temperature of 45-55 ℃ for 30-50min to obtain the heat-insulating layer 121.
6. The health-preserving medicinal liquor as claimed in claim 5, wherein the surfactant is one or a mixture of two or more of tween-60, tween-80 and polyether modified silicone oil in any proportion; the foaming agent is one or a mixture of more than two of dichloromethane, petroleum ether, n-pentane, isopentane and n-hexane in any proportion; the curing agent is a mixture of phosphoric acid and p-toluenesulfonic acid according to a mass ratio of 1: 2-4.
7. The health preserving medicinal liquor as claimed in claim 5, wherein the preparation method of the heat preserving and insulating resin is as follows:
b1: adding phenol into a four-neck flask provided with a stirrer, a reflux condenser tube, a thermometer and a constant-pressure dropping funnel, heating to melt the phenol, adding a formaldehyde aqueous solution after melting, dropwise adding a sodium hydroxide aqueous solution under the conditions that the temperature is 40-45 ℃ and the stirring speed is 800r/min, controlling the dropwise adding speed to be 1 drop/s, adjusting the temperature of a reaction system to be 50-55 ℃ after dropwise adding, reacting at a constant temperature for 1-3h, then heating to 80-85 ℃ and reacting at a constant temperature for 2-4h, after the reaction is finished, cooling in an ice water bath to be below 40 ℃, then adjusting the reaction product to be neutral by using acid, and then dehydrating the reaction product in vacuum to obtain an intermediate product A;
b2: adding the intermediate 1, chlorobenzene and potassium hydroxide into a three-neck flask provided with a stirrer, a gas-guide tube and a thermometer, introducing nitrogen for protection, dispersing the reaction system for 10-20min under the conditions of ice water bath and stirring speed of 2500-, stirring for 10-20min, performing rotary evaporation of the reaction product at 80-90 deg.C, dissolving the evaporation product in chloroform, then washing with hydrochloric acid solution and distilled water for 3-5 times, standing for layering, collecting organic phase, rotary evaporating at 80-90 deg.C, placing the evaporation product in vacuum drying oven, drying the mixture to constant weight at the temperature of 50-70 ℃ to obtain the heat-insulating resin.
8. The health preserving medicinal liquor as claimed in claim 7, wherein the mass fraction of the aqueous formaldehyde solution in step B1 is 35-38%, the mass fraction of the aqueous sodium hydroxide solution is 40-50%, and the molar ratio of phenol, formaldehyde and sodium hydroxide is 1.0: 1.6-1.8: 0.04-0.06, wherein the acid is one of hydrochloric acid, phosphoric acid, glacial acetic acid and p-toluenesulfonic acid.
9. A health preserving medicated wine as claimed in claim 7, wherein the dosage ratio of the intermediate 1, chlorobenzene, potassium hydroxide and phenyl dichlorophosphate solution in step B2 is 8 g: 12mL of: 3.5 g: 20mL, the phenyl dichloride solution is phenyl dichloride according to the weight ratio of 3.5 g: 10mL of solution formed by dissolving chlorobenzene, wherein the mass fraction of the hydrochloric acid solution is 10%.
10. The brewing method of the health preserving medicinal liquor as claimed in claim 1, which is characterized by comprising the following steps:
the method comprises the following steps: weighing 1 part of oyster, 1 part of spina date seed, 3 parts of medlar, 3 parts of ginseng, 4 parts of Chinese date, 2 parts of rhizoma polygonati, 3 parts of propolis, 3 parts of cervus elaphus linnaeus, 2 parts of gecko, 3 parts of cervus elaphus linnaeus embryo, 3 parts of astragalus, 2 parts of dendrobe, 2 parts of epimedium, 2 parts of semen cuscutae, 1 part of ginkgo leaf, 3 parts of honey, 1 part of semen coicis, 1 part of arillus longan, 2 parts of liquorice, 1 part of cinnamon, 2 parts of phaseolus calcaratus, 3 parts of endothelium corneum gigeriae galli, 2 parts of fructus alpiniae oxyphyllae, 1 part of honeysuckle and 3 parts of radix puerariae according to parts by weight for later use;
step two: mixing Concha Ostreae, propolis, cornu Cervi Pantotrichum, Gecko, embryo Cervi, Mel, and endothelium corneum Gigeriae Galli to obtain Chinese medicinal mixture A;
step three: mixing semen Ziziphi Spinosae, fructus Lycii, Ginseng radix, fructus Jujubae, rhizoma Polygonati, radix astragali, herba Dendrobii, herba Epimedii, semen Cuscutae, folium Ginkgo, Coicis semen, arillus longan, Glycyrrhrizae radix, cortex Cinnamomi, semen Phaseoli, fructus Alpinae Oxyphyllae, flos Lonicerae, and radix Puerariae to obtain Chinese medicinal mixture B;
step four: respectively adding hot water from a heat recovery chamber into the traditional Chinese medicine mixture A and the traditional Chinese medicine mixture B, soaking for 12h, taking out the traditional Chinese medicine mixture A, steaming for 60 min on strong fire, cooling for later use, taking out the traditional Chinese medicine mixture B, putting into a container, boiling for 30min on strong fire, and cooling for later use;
step five: adding 60-degree Chinese liquor into the steamed Chinese medicinal mixture A and the boiled Chinese medicinal mixture B respectively, and soaking for 15 days;
step six: putting the Chinese medicinal mixture A, the Chinese medicinal mixture B, the Chinese medicinal soaking solution, the water soaking solution and the wine grain after soaking in the white wine into a cellar pool for fermenting for 90 days to obtain a fermented material;
step seven: adding the fermented material into a brewing distiller (102) of a medicated wine brewing device, spraying fire into an inner cavity of a combustion chamber (105) through a flame sprayer (106) to heat the brewing distiller (102), heating the brewing distiller (102) to distill the fermented material, enabling alcohol to form alcohol vapor to rise, entering a return pipe (107), liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller (102), and enabling the rest of the alcohol vapor to enter a heat recovery chamber (104) through a vapor guide pipe (108);
step eight: cooling clean water is injected into the heat recovery chamber from the water inlet pipe (117), alcohol steam is shunted through the shunt pipe (109) and enters the plurality of condensation pipes (110), drops are formed by cooling of the cooling clean water, medicinal liquor is obtained, the medicinal liquor is converged through the confluence pipe (111), enters the guide pipe (113), enters the discharging pipe (114) through flow guiding, a valve is opened, the medicinal liquor is discharged from the discharging pipe (114) and collected in the collection tank (116), and sealing is carried out.
Background
The wine is called as 'the best of all drugs', the medicinal liquor which integrates the traditional Chinese medicines for strengthening the body and the wine is convenient to prepare, stable in medicine property, safe and effective, and various active ingredients of the traditional Chinese medicines are easily dissolved in the wine because the alcohol is a good semipolar organic solvent, so that the efficacy of the traditional Chinese medicines is fully exerted by the aid of the wine power and the wine assistant medicine potential, and the curative effect is improved.
Most of the existing medicinal liquor is produced by a soaking extraction process, which is not beneficial to large-scale production, and the prepared wine brewed by the method has obvious color and low human acceptance and affinity, and the drug molecules of the soaking extraction process are macromolecular structures, which are not beneficial to quick absorption by human bodies, and the drug effect is low and has toxicity.
Therefore, the key point of the invention is to provide a method for brewing the medicinal liquor, which can realize large-scale production, is energy-saving and environment-friendly in the production process and can reduce the cost, and the improvement of the medicinal effect of the medicinal liquor and the reduction of the drug toxicity.
Disclosure of Invention
In order to overcome the technical problems, the invention aims to provide a health preserving medicinal liquor and a brewing method thereof: the animal medicines and the plant medicines are soaked in boiling water, then the animal medicines are steamed and the plant medicines are boiled, then the animal medicines and the plant medicines are soaked in white wine, finally the animal medicines and the plant medicines are put into a cellar together with white wine soaking liquid, water soaking liquid and wine grains for fermentation, and a fermentation material is added into a wine brewing distiller of a wine brewing device for distillation to form the medicinal wine.
The purpose of the invention can be realized by the following technical scheme:
the health-preserving medicinal liquor comprises the following components in parts by weight:
1 part of oyster, 1 part of spina date seed, 3 parts of medlar, 3 parts of ginseng, 4 parts of Chinese date, 2 parts of rhizoma polygonati, 3 parts of propolis, 3 parts of cervus elaphus linnaeus, 2 parts of gecko, 3 parts of cervus elaphus linnaeus embryo, 3 parts of astragalus membranaceus, 2 parts of dendrobe, 2 parts of epimedium, 2 parts of semen cuscutae, 1 part of ginkgo leaf, 3 parts of honey, 1 part of semen coicis, 1 part of arillus longan, 2 parts of liquorice, 1 part of cinnamon, 2 parts of phaseolus calcaratus, 3 parts of endothelium corneum gigeriae galli, 2 parts of fructus alpiniae oxyphyllae, 1 part of honeysuckle and 3 parts of radix puerariae;
the medicinal liquor is prepared by the following steps:
the method comprises the following steps: mixing Concha Ostreae, propolis, cornu Cervi Pantotrichum, Gecko, embryo Cervi, Mel, and endothelium corneum Gigeriae Galli to obtain Chinese medicinal mixture A;
step two: mixing semen Ziziphi Spinosae, fructus Lycii, Ginseng radix, fructus Jujubae, rhizoma Polygonati, radix astragali, herba Dendrobii, herba Epimedii, semen Cuscutae, folium Ginkgo, Coicis semen, arillus longan, Glycyrrhrizae radix, cortex Cinnamomi, semen Phaseoli, fructus Alpinae Oxyphyllae, flos Lonicerae, and radix Puerariae to obtain Chinese medicinal mixture B;
step three: respectively adding hot water from a heat recovery chamber into the traditional Chinese medicine mixture A and the traditional Chinese medicine mixture B, soaking for 12h, taking out the traditional Chinese medicine mixture A, steaming for 60 min on strong fire, cooling for later use, taking out the traditional Chinese medicine mixture B, putting into a container, boiling for 30min on strong fire, and cooling for later use;
step four: adding 60-degree Chinese liquor into the steamed Chinese medicinal mixture A and the boiled Chinese medicinal mixture B respectively, and soaking for 15 days;
step five: putting the Chinese medicinal mixture A, the Chinese medicinal mixture B, the Chinese medicinal soaking solution, the water soaking solution and the wine grain after soaking in the white wine into a cellar pool for fermenting for 90 days to obtain a fermented material;
step six: adding the fermented material into a brewing distiller of a medicated wine brewing device, spraying fire into an inner cavity of a combustion chamber through a flame thrower to heat the brewing distiller, heating the brewing distiller to distill the fermented material, enabling alcohol to form alcohol vapor to rise, entering a return pipe, liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller, and enabling the rest alcohol vapor to enter a heat recovery chamber through a vapor conduit;
step seven: injecting cooling clear water into the heat recovery chamber from the water inlet pipe, shunting alcohol steam into the plurality of condensing pipes through the shunt pipes, cooling by the cooling clear water to form liquid drops to obtain medicinal liquor, converging the medicinal liquor through the collecting pipes, then entering the flow guide pipe, entering the discharging pipe through flow guide, opening the valve, discharging the medicinal liquor from the discharging pipe, collecting the medicinal liquor in the collecting tank, and sealing.
As a further scheme of the invention: the medicinal liquor brewing device comprises an installation base, a brewing distiller, a discharging box and a heat recovery chamber, wherein the discharging box is installed on one side of the installation base, the brewing distiller is embedded and installed on the installation base, and the heat recovery chamber is installed at the top of the discharging box;
the wine brewing device is characterized in that a combustion chamber is arranged in an inner cavity of the mounting base, a flame thrower is arranged at the bottom of the inner cavity of the combustion chamber and is positioned under the wine brewing distiller, a sealing door is rotatably arranged on one side of the discharging box, a sterile chamber is arranged in the inner cavity of the discharging box, a collecting tank is arranged in the inner cavity of the sterile chamber and is positioned under a discharging pipe, a valve is arranged on the discharging pipe, the discharging pipe is arranged at the bottom end of a flow guide pipe, the discharging pipe is arranged at the top of the discharging box in a penetrating manner, a return pipe is arranged at the top of the wine brewing distiller, a steam guide pipe is arranged at the top end of the return pipe, one end, away from the return pipe, of the steam guide pipe penetrates through the top of the heat recovery chamber and is connected to the top of the flow guide pipe, a plurality of condensation pipes are arranged at equal intervals at the bottom of the flow guide pipe, the condensation pipes are S-shaped, and the bottom ends of the condensation pipes are communicated to the top of the flow guide pipe, the two ends of the flow dividing pipe and the two ends of the collecting pipe are respectively arranged on the two sides of the inner wall of the heat recovery chamber, the bottom of the collecting pipe is provided with a flow guide hopper, and the bottom end of the flow guide hopper is communicated to the top end of the flow guide pipe.
As a further scheme of the invention: the inlet tube is installed at the one end top of heat recovery room, drain pipe and gas release pipe are installed to one side bottom of heat recovery room, the gas release pipe is installed and is served at the drainage fill, the gas release pipe becomes arc and port up.
As a further scheme of the invention: the heat recovery chamber is formed by the concatenation of a plurality of composite sheet, the composite sheet includes first stainless steel layer, thermal insulation layer, second stainless steel layer, the thermal insulation layer is located the position between first stainless steel layer, the second stainless steel layer, and thermal insulation layer and the equal fixed connection of first stainless steel layer, second stainless steel layer.
As a further scheme of the invention: the preparation method of the heat preservation and insulation layer comprises the following steps
A1: weighing 100-200 parts of heat-insulating resin, 3.5-7.0 parts of surfactant, 6-12 parts of foaming agent and 15-21 parts of curing agent according to parts by weight for later use;
a2: adding the heat-preservation and heat-insulation resin and the surfactant into a high-speed dispersing machine, and uniformly mixing to obtain a mixture A;
a3: adding a foaming agent into the mixture A for continuous dispersion, and uniformly mixing to obtain a mixture B;
a4: and adding the curing agent into the mixture B for continuous dispersion, uniformly mixing, pouring into a preheated mold, placing the mold in a constant-temperature oven at the temperature of 75-80 ℃ for drying for 10-20min, taking out the mold, and curing at the temperature of 45-55 ℃ for 30-50min to obtain the heat-insulating layer 121.
As a further scheme of the invention: the surfactant is one or a mixture of more than two of Tween-60, Tween-80 and polyether modified silicone oil according to any proportion; the foaming agent is one or a mixture of more than two of dichloromethane, petroleum ether, n-pentane, isopentane and n-hexane in any proportion; the curing agent is a mixture of phosphoric acid and p-toluenesulfonic acid according to a mass ratio of 1: 2-4.
As a further scheme of the invention: the preparation method of the heat preservation and insulation resin comprises the following steps:
b1: adding phenol into a four-neck flask provided with a stirrer, a reflux condenser tube, a thermometer and a constant-pressure dropping funnel, heating to melt the phenol, adding a formaldehyde aqueous solution after melting, dropwise adding a sodium hydroxide aqueous solution under the conditions that the temperature is 40-45 ℃ and the stirring speed is 800r/min, controlling the temperature of a reaction system to be not higher than 60 ℃ and the dropping speed to be 1 drop/s, adjusting the temperature of the reaction system to be 50-55 ℃ after dropwise adding, reacting at a constant temperature for 1-3h, then heating to 80-85 ℃ and reacting at a constant temperature for 2-4h, finishing the reaction, cooling in an ice water bath to be below 40 ℃, then adjusting a reaction product to be neutral by using acid, and then dehydrating the reaction product in vacuum to obtain an intermediate product A;
the reaction principle is as follows:
b2: adding the intermediate 1, chlorobenzene and potassium hydroxide into a three-neck flask provided with a stirrer, a gas-guide tube and a thermometer, introducing nitrogen for protection, dispersing the reaction system for 10-20min under the conditions of ice water bath and stirring speed of 2500-, stirring for 10-20min, performing rotary evaporation of the reaction product at 80-90 deg.C, dissolving the evaporation product in chloroform, then washing with hydrochloric acid solution and distilled water for 3-5 times, standing for layering, collecting organic phase, rotary evaporating at 80-90 deg.C, placing the evaporation product in vacuum drying oven, drying the mixture to constant weight at the temperature of 50-70 ℃ to obtain the heat-insulating resin.
The reaction principle is as follows:
as a further scheme of the invention: in the step B1, the mass fraction of the formaldehyde aqueous solution is 35-38%, the mass fraction of the sodium hydroxide aqueous solution is 40-50%, and the molar ratio of phenol to formaldehyde to sodium hydroxide is 1.0: 1.6-1.8: 0.04-0.06, wherein the acid is one of hydrochloric acid, phosphoric acid, glacial acetic acid and p-toluenesulfonic acid.
As a further scheme of the invention: the dosage ratio of the intermediate 1, chlorobenzene, potassium hydroxide and phenyl dichlorophosphate solution in the step B2 is 8 g: 12mL of: 3.5 g: 20mL, the phenyl dichloride solution is phenyl dichloride according to the weight ratio of 3.5 g: 10mL of solution formed by dissolving chlorobenzene, wherein the mass fraction of the hydrochloric acid solution is 10%.
As a further scheme of the invention: a brewing method of health-preserving medicinal liquor comprises the following steps:
the method comprises the following steps: weighing 1 part of oyster, 1 part of spina date seed, 3 parts of medlar, 3 parts of ginseng, 4 parts of Chinese date, 2 parts of rhizoma polygonati, 3 parts of propolis, 3 parts of cervus elaphus linnaeus, 2 parts of gecko, 3 parts of cervus elaphus linnaeus embryo, 3 parts of astragalus, 2 parts of dendrobe, 2 parts of epimedium, 2 parts of semen cuscutae, 1 part of ginkgo leaf, 3 parts of honey, 1 part of semen coicis, 1 part of arillus longan, 2 parts of liquorice, 1 part of cinnamon, 2 parts of phaseolus calcaratus, 3 parts of endothelium corneum gigeriae galli, 2 parts of fructus alpiniae oxyphyllae, 1 part of honeysuckle and 3 parts of radix puerariae according to parts by weight for later use;
step two: mixing Concha Ostreae, propolis, cornu Cervi Pantotrichum, Gecko, embryo Cervi, Mel, and endothelium corneum Gigeriae Galli to obtain Chinese medicinal mixture A;
step three: mixing semen Ziziphi Spinosae, fructus Lycii, Ginseng radix, fructus Jujubae, rhizoma Polygonati, radix astragali, herba Dendrobii, herba Epimedii, semen Cuscutae, folium Ginkgo, Coicis semen, arillus longan, Glycyrrhrizae radix, cortex Cinnamomi, semen Phaseoli, fructus Alpinae Oxyphyllae, flos Lonicerae, and radix Puerariae to obtain Chinese medicinal mixture B;
step four: respectively adding hot water from a heat recovery chamber into the traditional Chinese medicine mixture A and the traditional Chinese medicine mixture B, soaking for 12h, taking out the traditional Chinese medicine mixture A, steaming for 60 min on strong fire, cooling for later use, taking out the traditional Chinese medicine mixture B, putting into a container, boiling for 30min on strong fire, and cooling for later use;
step five: adding 60-degree Chinese liquor into the steamed Chinese medicinal mixture A and the boiled Chinese medicinal mixture B respectively, and soaking for 15 days;
step six: putting the Chinese medicinal mixture A, the Chinese medicinal mixture B, the Chinese medicinal soaking solution, the water soaking solution and the wine grain after soaking in the white wine into a cellar pool for fermenting for 90 days to obtain a fermented material;
step seven: adding the fermented material into a brewing distiller of a medicated wine brewing device, spraying fire into an inner cavity of a combustion chamber through a flame thrower to heat the brewing distiller, heating the brewing distiller to distill the fermented material, enabling alcohol to form alcohol vapor to rise, entering a return pipe, liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller, and enabling the rest alcohol vapor to enter a heat recovery chamber through a vapor conduit;
step eight: injecting cooling clear water into the heat recovery chamber from the water inlet pipe, shunting alcohol steam into the plurality of condensing pipes through the shunt pipes, cooling by the cooling clear water to form liquid drops to obtain medicinal liquor, converging the medicinal liquor through the collecting pipes, then entering the flow guide pipe, entering the discharging pipe through flow guide, opening the valve, discharging the medicinal liquor from the discharging pipe, collecting the medicinal liquor in the collecting tank, and sealing.
The invention has the beneficial effects that:
the invention relates to a health preserving medicinal liquor and a brewing method thereof, which comprises the steps of soaking animal medicines and plant medicines in boiling water, steaming the animal medicines and the plant medicines, boiling the animal medicines and the plant medicines, soaking the animal medicines and the plant medicines in white wine, fermenting the animal medicines, the plant medicines, the white wine and the white wine in a cellar together, adding a fermentation material into a brewing distiller of a medicinal liquor brewing device, heating the brewing distiller by a flame sprayer, heating the brewing distiller to distill the fermentation material, leading alcohol to form alcohol vapor to rise, entering a return pipe, liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller, leading the rest alcohol vapor to enter a heat recovery chamber through a vapor conduit, injecting cooling clear water into the heat recovery chamber from a water inlet pipe, shunting the alcohol vapor to a plurality of condensing pipes through shunt pipes, and cooling the alcohol vapor to form liquid drops, thus obtaining the medicinal liquor, the medicinal liquor is converged by a collecting pipe and then enters a flow guide pipe, and then enters a discharging pipe through flow guide, a valve is opened, the medicinal liquor is discharged from the discharging pipe and collected in a collecting tank, and the collecting tank is sealed; the medicinal liquor has high purity, is colorless, transparent, slightly medicinal, good in taste and good in appearance, is prepared by replacing the traditional soaking production process with a fermentation distillation process, is changed into colorless and transparent liquid from the traditional yellow color, improves the acceptance and affinity of people, changes the molecular structure of the medicine in the fermentation process, ensures that the medicine molecules in the soaking extraction process are in a macromolecular structure, decomposes the medicine molecules into small molecular structures by the fermentation distillation process, is beneficial to the quick absorption of a human body, improves the effect of the medicine, and simultaneously eliminates the toxicity of the medicine.
The medicinal liquor brewing device is characterized in that cooling clear water is injected into the heat recovery chamber to rapidly condense alcohol vapor to form medicinal liquor, heat in the process of liquefying the alcohol vapor is absorbed by the cooling clear water, the cooling clear water is heated and then can be used for soaking raw materials, also can be used for steaming animal medicines and boiling plant medicines, and hot water is used for replacing cooling to reduce energy consumption, so that the energy-saving effect is realized, the cooling water resource has reasonable use, and the waste of water resources is reduced; the heat recovery chamber is formed by splicing a plurality of composite boards, each composite board comprises a first stainless steel layer, a heat insulation layer and a second stainless steel layer, the edible stainless steel layer is used for containing water, the safety is high, the heat insulation layers are used for heat insulation and heat preservation, the phenol and formaldehyde react and polymerize to form a high polymer material, the material has a large number of benzene rings and good temperature resistance, the material is modified by phenyl dichlorophosphate, so that phosphorus is introduced into a high polymer chain to form a chemical bond with high bond energy, the heat resistance of the material is further improved, the modified high polymer material is made into a foam material, the heat transfer performance of the foam material is low, the foam contains a large amount of air, the movement of the air is seriously hindered, and the air and micropores in the foam material prevent the convection heat conduction effect formed by the circulation of the air, can play fine heat preservation effect, reduce the energy and outwards conduct and waste for the heat can be fully absorbed by cold clear water cooling clear water, and can not destroyed when 300 ℃, can normal use, therefore this medicinal liquor brewing device is used for the preparation of this medicinal liquor, not only can promote the medicine effect, promotes the product quality, accomplishes energy-concerving and environment-protective still, reduction in production cost.
Drawings
The invention will be further described with reference to the accompanying drawings.
FIG. 1 is a schematic structural view of a brewing apparatus for medicated wine according to the present invention;
FIG. 2 is an interior side view of the heat recovery chamber of the present invention;
fig. 3 is an enlarged schematic view of fig. 1 at a in the present invention.
In the figure: 101. installing a base; 102. a wine brewing distiller; 103. a material placing box; 104. a heat recovery chamber; 105. a combustion chamber; 106. a flame thrower; 107. a return pipe; 108. a steam conduit; 109. a shunt tube; 110. a condenser tube; 111. a collector pipe; 112. a flow guide hopper; 113. a flow guide pipe; 114. discharging the material pipe; 115. a sterile room; 116. a collection tank; 117. a water inlet pipe; 118. a drain pipe; 119. discharging the air pipe; 120. a first stainless steel layer; 121. a heat insulation layer; 122. a second stainless steel layer.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
referring to fig. 1-3, the present embodiment is a medicated wine brewing apparatus, including an installation base 101, a brewing distiller 102, a material discharge box 103, and a heat recovery chamber 104, wherein the material discharge box 103 is installed on one side of the installation base 101, the brewing distiller 102 is embedded in the installation base 101, and the heat recovery chamber 104 is installed on the top of the material discharge box 103;
the wine brewing device is characterized in that a combustion chamber 105 is arranged in an inner cavity of the mounting base 101, a flame thrower 106 is arranged at the bottom of the inner cavity of the combustion chamber 105, the flame thrower 106 is positioned under the wine brewing distiller 102, a sealing door is rotatably arranged on one side of the discharging box 103, an aseptic chamber 115 is arranged in the inner cavity of the discharging box 103, a collecting tank 116 is placed in the inner cavity of the aseptic chamber 115, the collecting tank 116 is positioned under a discharging pipe 114, a valve is arranged on the discharging pipe 114, the discharging pipe 114 is arranged at the bottom end of a guide pipe 113, the discharging pipe 114 is arranged at the top of the discharging box 103 in a penetrating manner, a return pipe 107 is arranged at the top of the wine brewing distiller 102, a steam guide pipe 108 is arranged at the top end of the return pipe 107, one end, far away from the return pipe 108, penetrates through the top of the heat recovery chamber 104 and is connected to the top of the shunt pipe 109, and a plurality of condensing pipes 110 are equidistantly arranged at the bottom of the shunt pipe 109, the condenser tubes 110 are S-shaped, the bottom ends of the condenser tubes 110 are all communicated to the top of the collecting tube 111, two ends of the shunt tube 109 and the collecting tube 111 are respectively installed on two sides of the inner wall of the heat recovery chamber 104, the bottom of the collecting tube 111 is provided with a flow guide hopper 112, and the bottom end of the flow guide hopper 112 is communicated to the top end of the flow guide tube 113.
An inlet pipe 117 is installed at the top of one end of the heat recovery chamber 104, a drain pipe 118 and an air release pipe 119 are installed at the bottom of one side of the heat recovery chamber 104, the air release pipe 119 is installed at one end of the flow guide hopper 112, and the air release pipe 119 is arc-shaped and has an upward port.
The heat recovery chamber 104 is formed by splicing a plurality of composite plates, each composite plate comprises a first stainless steel layer 120, a heat-insulating layer 121 and a second stainless steel layer 122, the heat-insulating layer 121 is located between the first stainless steel layer 120 and the second stainless steel layer 122, and the heat-insulating layer 121 is fixedly connected with the first stainless steel layer 120 and the second stainless steel layer 122.
Example 2:
the embodiment is a preparation method of a heat preservation and insulation layer 121, which comprises the following steps:
s1: adding phenol into a four-neck flask provided with a stirrer, a reflux condenser tube, a thermometer and a constant-pressure dropping funnel, heating to melt the phenol, adding a formaldehyde aqueous solution after melting, dropwise adding a sodium hydroxide aqueous solution under the conditions that the temperature is 40 ℃ and the stirring speed is 500r/min, controlling the temperature of a reaction system to be not higher than 60 ℃ and the dropping speed to be 1 drop/s, adjusting the temperature of the reaction system to be 50 ℃ after dropwise adding, reacting for 1 hour at constant temperature, then heating to 80 ℃ and reacting for 2 hours at constant temperature, after the reaction is finished, cooling in an ice water bath to be below 40 ℃, then adjusting the reaction product to be neutral by using acid, and then carrying out vacuum dehydration on the reaction product to obtain an intermediate product A; controlling the mass fraction of the formaldehyde aqueous solution to be 35%, the mass fraction of the sodium hydroxide aqueous solution to be 40%, and the molar ratio of the phenol to the formaldehyde to the sodium hydroxide to be 1.0: 1.6: 0.04, wherein the acid is hydrochloric acid;
s2: adding the intermediate 1, chlorobenzene and potassium hydroxide into a three-neck flask provided with a stirrer, an air guide pipe and a thermometer, introducing nitrogen for protection, dispersing a reaction system for 10min under the condition of ice water bath and the stirring speed of 2500r/min, adding phenyl dichlorophosphate solution into the three-neck flask, continuously stirring for 10min, after the reaction is finished, carrying out rotary evaporation on a reaction product at the temperature of 80 ℃, dissolving the evaporation product into chloroform, respectively washing for 3 times with hydrochloric acid solution and distilled water, standing for layering, collecting an organic phase, carrying out rotary evaporation on the organic phase at the temperature of 80 ℃, placing the evaporation product into a vacuum drying oven, and drying to constant weight at the temperature of 50 ℃ to obtain heat-insulating resin; controlling the dosage ratio of the intermediate 1, chlorobenzene, potassium hydroxide and phenyl dichlorophosphate solution to be 8 g: 12mL of: 3.5 g: 20mL, the phenyl dichloride solution is phenyl dichloride according to the weight ratio of 3.5 g: 10mL of solution formed by dissolving chlorobenzene, wherein the mass fraction of the hydrochloric acid solution is 10%.
S3: weighing 100 parts of heat-insulating resin, 3.5 parts of surfactant, 6 parts of foaming agent and 15 parts of curing agent according to parts by weight for later use; the surfactant is tween-80; the foaming agent is n-hexane; the curing agent is a mixture of phosphoric acid and p-toluenesulfonic acid according to a mass ratio of 1: 4;
s4: adding the heat-preservation and heat-insulation resin and the surfactant into a high-speed dispersing machine, and uniformly mixing to obtain a mixture A;
s5: adding a foaming agent into the mixture A for continuous dispersion, and uniformly mixing to obtain a mixture B;
s6: and adding the curing agent into the mixture B for continuous dispersion, uniformly mixing, pouring into a preheated mold, placing the mold in a constant-temperature oven at the temperature of 75 ℃ for drying for 10min, taking out the mold, and curing at the temperature of 45 ℃ for 30min to obtain the heat-insulating layer 121.
The thermal insulation performance of the thermal insulation layer is tested by a thermal conductivity tester, and the specific method refers to GB/T10801 (polystyrene foam for thermal insulation), and the detection result shows that the thermal conductivity of the thermal insulation layer 121 is 0.021W/m.k.
Example 3:
the embodiment is a preparation method of a heat preservation and insulation layer 121, which comprises the following steps:
s1: adding phenol into a four-neck flask provided with a stirrer, a reflux condenser tube, a thermometer and a constant-pressure dropping funnel, heating to melt the phenol, adding a formaldehyde aqueous solution after melting, dropwise adding a sodium hydroxide aqueous solution under the conditions that the temperature is 45 ℃ and the stirring speed is 800r/min, controlling the temperature of a reaction system to be not higher than 60 ℃, controlling the dropwise adding speed to be 1 drop/s, adjusting the temperature of the reaction system to be 55 ℃ after dropwise adding, reacting for 3 hours at constant temperature, then heating to 85 ℃ and reacting for 4 hours at constant temperature, after the reaction, cooling to below 40 ℃ in an ice water bath, then adjusting the reaction product to be neutral by using acid, and then carrying out vacuum dehydration on the reaction product to obtain an intermediate product A; controlling the mass fraction of the formaldehyde aqueous solution to be 38%, the mass fraction of the sodium hydroxide aqueous solution to be 50%, and the molar ratio of the phenol to the formaldehyde to the sodium hydroxide to be 1.0: 1.8: 0.04-0.06, wherein the acid is glacial acetic acid;
s2: adding the intermediate 1, chlorobenzene and potassium hydroxide into a three-neck flask provided with a stirrer, an air guide pipe and a thermometer, introducing nitrogen for protection, dispersing a reaction system for 20min under the condition of ice water bath and the stirring speed of 5000r/min, adding phenyl dichlorophosphate solution into the three-neck flask, continuously stirring for 20min, after the reaction is finished, carrying out rotary evaporation on a reaction product at the temperature of 90 ℃, dissolving the evaporation product in chloroform, respectively washing for 3-5 times with hydrochloric acid solution and distilled water, standing for layering, collecting an organic phase, carrying out rotary evaporation on the organic phase at the temperature of 90 ℃, placing the evaporation product in a vacuum drying oven, and drying to constant weight at the temperature of 70 ℃ to obtain heat-insulating resin; controlling the dosage ratio of the intermediate 1, chlorobenzene, potassium hydroxide and phenyl dichlorophosphate solution to be 8 g: 12mL of: 3.5 g: 20mL, the phenyl dichloride solution is phenyl dichloride according to the weight ratio of 3.5 g: 10mL of solution formed by dissolving chlorobenzene, wherein the mass fraction of the hydrochloric acid solution is 10%.
S3: weighing 200 parts of heat-insulating resin, 7.0 parts of surfactant, 12 parts of foaming agent and 21 parts of curing agent according to parts by weight for later use; the surfactant is tween-60; the foaming agent is a mixture of dichloromethane and n-hexane according to a mass ratio of 1: 1; the curing agent is a mixture of phosphoric acid and p-toluenesulfonic acid according to a mass ratio of 1: 2;
s4: adding the heat-preservation and heat-insulation resin and the surfactant into a high-speed dispersing machine, and uniformly mixing to obtain a mixture A;
s5: adding a foaming agent into the mixture A for continuous dispersion, and uniformly mixing to obtain a mixture B;
s6: and adding the curing agent into the mixture B for continuous dispersion, uniformly mixing, pouring into a preheated mold, placing the mold in a constant-temperature oven at the temperature of 80 ℃ for drying for 20min, taking out the mold, and curing for 50min at the temperature of 55 ℃ to obtain the heat-insulating layer 121.
The thermal insulation performance of the thermal insulation layer is tested by a thermal conductivity tester, and the specific method refers to GB/T10801 (polystyrene foam for thermal insulation), and the detection result shows that the thermal conductivity of the thermal insulation layer 121 is 0.016W/m.k.
Example 4:
referring to fig. 1-3, the present embodiment is a method for brewing health preserving medicated wine, including the following steps:
the method comprises the following steps: weighing 1 part of oyster, 1 part of spina date seed, 3 parts of medlar, 3 parts of ginseng, 4 parts of Chinese date, 2 parts of rhizoma polygonati, 3 parts of propolis, 3 parts of cervus elaphus linnaeus, 2 parts of gecko, 3 parts of cervus elaphus linnaeus embryo, 3 parts of astragalus, 2 parts of dendrobe, 2 parts of epimedium, 2 parts of semen cuscutae, 1 part of ginkgo leaf, 3 parts of honey, 1 part of semen coicis, 1 part of arillus longan, 2 parts of liquorice, 1 part of cinnamon, 2 parts of phaseolus calcaratus, 3 parts of endothelium corneum gigeriae galli, 2 parts of fructus alpiniae oxyphyllae, 1 part of honeysuckle and 3 parts of radix puerariae according to parts by weight for later use;
step two: mixing Concha Ostreae, propolis, cornu Cervi Pantotrichum, Gecko, embryo Cervi, Mel, and endothelium corneum Gigeriae Galli to obtain Chinese medicinal mixture A;
step three: mixing semen Ziziphi Spinosae, fructus Lycii, Ginseng radix, fructus Jujubae, rhizoma Polygonati, radix astragali, herba Dendrobii, herba Epimedii, semen Cuscutae, folium Ginkgo, Coicis semen, arillus longan, Glycyrrhrizae radix, cortex Cinnamomi, semen Phaseoli, fructus Alpinae Oxyphyllae, flos Lonicerae, and radix Puerariae to obtain Chinese medicinal mixture B;
step four: respectively adding hot water from a heat recovery chamber into the traditional Chinese medicine mixture A and the traditional Chinese medicine mixture B, soaking for 12h, taking out the traditional Chinese medicine mixture A, steaming for 60 min on strong fire, cooling for later use, taking out the traditional Chinese medicine mixture B, putting into a container, boiling for 30min on strong fire, and cooling for later use;
step five: adding 60-degree Chinese liquor into the steamed Chinese medicinal mixture A and the boiled Chinese medicinal mixture B respectively, and soaking for 15 days;
step six: putting the Chinese medicinal mixture A, the Chinese medicinal mixture B, the Chinese medicinal soaking solution, the water soaking solution and the wine grain after soaking in the white wine into a cellar pool for fermenting for 90 days to obtain a fermented material;
step seven: adding the fermented material into a brewing distiller 102 of a medicated wine brewing device, flaming the fermented material into an inner cavity of a combustion chamber 105 through a flame thrower 106 to heat the brewing distiller 102, heating the brewing distiller 102 to distill the fermented material, rising alcohol to form alcohol vapor, entering a return pipe 107, liquefying part of the alcohol vapor to form liquid drops, returning the liquid drops to the brewing distiller 102, and entering the rest alcohol vapor into a heat recovery chamber 104 through a vapor conduit 108;
step eight: cooling clean water is injected into the heat recovery chamber from the water inlet pipe 117, alcohol steam is shunted through the shunt pipes 109 and enters the plurality of condensing pipes 110, drops are formed by cooling of the cooling clean water, medicinal liquor is obtained, the medicinal liquor is converged through the collecting pipe 111 and then enters the guide pipe 113, the medicinal liquor enters the discharging pipe 114 through diversion, the valve is opened, the medicinal liquor is discharged from the discharging pipe 114 and collected in the collection tank 116, and sealing is carried out.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing is illustrative and explanatory only and is not intended to be exhaustive or to limit the invention to the precise embodiments described, and various modifications, additions, and substitutions may be made by those skilled in the art without departing from the scope of the invention or exceeding the scope of the claims.
- 上一篇:石墨接头机器人自动装卡簧、装栓机
- 下一篇:一种SOD白酒制造方法