1. The synergist is characterized by being prepared from the following components in parts by weight: 20-40 parts of 4-methylbenzene hydrazide, 20-40 parts of sodium bicarbonate, 5-10 parts of alumina, 10-15 parts of monosulfonate and 300 parts of distilled water.

2. A process for preparing a synergist, which comprises the steps of preparing 20-40 parts of 4-methylbenzenesulfonic hydrazide, 20-40 parts of sodium bicarbonate, 5-10 parts of alumina, 10-15 parts of monosulfonate and 300 parts of distilled water according to claim 1 by using a preparation device which comprises a support component (100), a transmission component (200) and a reaction vessel (300) and can change the posture according to the preparation steps.

3. The method according to claim 2, wherein the support assembly (100) comprises a base (110), at least two cross-members (120) spaced apart from each other on the base (110), and a limiting member (130) for limiting the position of the reaction vessel (300),

the limiting part (130) comprises a limiting groove (131) arranged on one side, far away from the ground, of the two ends of the limiting part (130), the limiting groove (131) is matched with the end part of the reaction container (300), under the condition that the limiting groove (131) is clamped with the first end (310) of the reaction container (300), the second end (320), which is not clamped with the limiting groove (131), of the reaction container (300) is in circular motion in the vertical direction based on the force transmitted by the transmission assembly (200) and the first end (310) serving as an origin, so that the reaction container (300) is gradually converted into an upright posture from a lying posture.

4. The manufacturing method according to claim 2, wherein the driving assembly (200) comprises a power unit (210), a first slide block (230) connected to the power unit (210) and driven by the power unit (210), a first slide slot (220) engaged with the first slide block (230) for guiding the first slide block (230) to move in a horizontal direction, a second slide slot (240) vertically connected to the first slide block (230), a second slide block (250) engaged with the second slide slot (240) and guided by the second slide slot (240) to move in a direction perpendicular to the ground, and a driving rod (260) for connecting the second slide block (250) and the reaction vessel (300),

when the first sliding block (230) is driven by the power device (210) to move along the guiding direction of the first sliding chute (220), the second sliding block (250) moves along the guiding direction of the second sliding chute (240) under the action of the pull force generated by the second sliding block (250) by the transmission rod (260) based on the gravity of the reaction container (300), and provides the pull force for the reaction container (300) so as to convert the lying posture into the vertical posture.

5. The method according to claim 2, wherein the reaction vessel (300) is provided with a pair of movable wheels (330) capable of engaging with the limiting grooves (131) at least at the first end (310) and the second end (320), respectively, the movable wheels (330) abut against the limiting member (130) and slide on the limiting grooves (131) at the two ends of the limiting member (130) at a distance therebetween under the driving of the transmission device,

when the movable wheel (330) at the second end (320) is engaged with the limiting groove (131) corresponding to the pulley at the second end (320) on the limiting member (130), the first end (310) of the reaction container (300) performs circular arc motion by taking the movable wheel (330) at the second end (320) as a circle center and taking the height of the reaction container (300) as a radius, so that the reaction container (300) is converted into an upright posture from a lying posture.

6. The method according to claim 5, wherein the reaction vessel (300) further comprises a degassing assembly, the degassing assembly at least comprises a degassing tube, a degassing pump and a degassing port, the degassing port is arranged on the side of the reaction vessel (300) far away from the ground when the reaction vessel is in the lying posture and is used for connecting the degassing pump, one end of the degassing port opposite to the degassing pump is connected with the degassing tube,

the degassing tube is provided with a sealing assembly in such a way as to prevent the entry of reactive substances into the degassing tube when the reaction vessel (300) is in an upright position.

7. The production method according to claim 6, wherein the reaction vessel further comprises a sterilization assembly including a jacket provided with a steam inlet, the jacket being provided at a lower portion near the ground when the reaction vessel (300) is in an upright posture in such a manner as to form a receiving space for receiving steam with an outer wall of the reaction vessel (300),

when the reaction vessel (300) is in an upright posture, the steam inlet of the jacket is arranged at one end of the jacket far away from the ground in a manner of preventing the backflow of condensed water.

8. The manufacturing method according to claim 7, wherein the reaction vessel further comprises a control module connected to a degassing assembly, a sterilizing assembly and a driving assembly (200), wherein when the degassing assembly is in an operating state, the control module controls the driving assembly (200) to operate to maintain the reaction vessel (300) in a lying state;

when the sterilization assembly is in the working state, the control module controls the transmission assembly (200) to work so as to keep the reaction vessel (300) in the vertical posture.

9. The preparation method according to claim 8, characterized in that the preparation device comprises a stirring shaft (375), the stirring shaft (375) is provided with at least two stirring fulcrum shafts (377) according to a mode capable of increasing the stirring performance of the preparation device, at least one stirring fulcrum shaft (377) is provided with asymmetrically arranged stirring blades (376), the stirring blades (376) are provided with at least three through holes (378) which are distributed in a disordered way,

with the preparation device in a lying position and the stirring shaft (375) rotated, the stirring blade (376) passes through the liquid in the preparation device, and the liquid in contact with the stirring blade (376) passes through the through-hole (378) under the action of pressure and gravity to form turbulent flow inside the preparation device.

10. Preparation method according to one of the preceding claims, characterized in that it comprises the following steps:

s1: the control module controls the temperature to be kept at 20-30 ℃, 30 parts of 4-methylbenzenesulfonic acid hydrazide, 30 parts of sodium bicarbonate, 8 parts of alumina, 12 parts of monosulfonate and 200 parts of distilled water are added into the reaction container (300), and the control module controls the transmission assembly (200) to work so as to convert the reaction container (300) from an upright posture to a lying posture;

s2: the control module controls the stirring assembly (370) to work so as to heat and stir the added substances for 3 hours;

s3: the control module controls the temperature of the reaction container to be reduced to 11-15 ℃, and controls the degassing component to work to degas the substances in the reaction container for 3-7 minutes;

s4: the control module controls the transmission assembly (200) to work, so that the reaction container (300) is converted from a lying posture to an upright posture, the sterilization assembly is controlled to start working, and sterilization is carried out for 15-20 minutes.

Background

The thickened oil contains less light fraction, high content of colloid and asphalt and higher viscosity. The mining rate of adopting the trying means is difficult in the bottom-crossing mining process, and the method of steam huff and puff can improve the mining rate of the thickened oil by 40 percent through steam driving. According to domestic thermal recovery practice in the last two decades, the steam huff and puff method also exposes a plurality of problems to be solved urgently, such as; the normal production of the heavy oil is disturbed by the improvement of the sweep coefficient of the steam in the steam flooding process, the physical properties of an oil reservoir and an oil layer, the recovery of condensed water in the huff and puff process, the lifting and gathering of the heavy oil at low temperature and the like.

In recent years, in order to overcome the problem of exposure of thick oil in the steam injection thermal recovery process, flue gas-steam compound flooding is adopted successively, a surfactant front-mounted slug is added before steam injection, nitrogen gas-surfactant foam flooding is adopted, urea is utilized to generate carbon dioxide and ammonia through thermal decomposition at high temperature, and steam-foam-weak base compound flooding and the like are formed by matching with a surfactant, so that the steam injection thermal recovery effect of the thick oil is enhanced to a certain extent, and the thick oil recovery degree is improved. However, these methods still have some disadvantages, such as: the corrosion of flue gas to a pipe column in the flue gas-steam combined flooding, the poor foaming capacity in the steam-surfactant flooding process, the high investment of a nitrogen generator in the implementation process of the nitrogen-surfactant foam flooding, and the balance of carbon dioxide, ammonia and water in the urea-surfactant foam flooding, when the temperature is reduced, the carbon dioxide and the ammonia react to generate ammonium carbonate and the like, so that the application of the ammonia-nitrogen combined flooding is limited.

Furthermore, on the one hand, due to the differences in understanding to the person skilled in the art; on the other hand, since the inventor has studied a lot of documents and patents when making the present invention, but the space is not limited to the details and contents listed in the above, however, the present invention is by no means free of the features of the prior art, but the present invention has been provided with all the features of the prior art, and the applicant reserves the right to increase the related prior art in the background.

Disclosure of Invention

Aiming at the defects of the prior art, the invention provides a synergist capable of promoting the oil extraction efficiency by a steam method.

The invention provides a synergist, which is prepared from the following components in parts by weight: 20-40 parts of 4-methylbenzene hydrazide, 20-40 parts of sodium bicarbonate, 5-10 parts of alumina, 10-15 parts of monosulfonate and 300 parts of distilled water.

The invention provides a preparation method of a synergist, which is prepared by adopting the components through a preparation device which comprises a reaction vessel, a supporting component and a transmission component and can be changed between lying and standing postures.

According to a preferred embodiment, the supporting part includes the base, two piece at least intervals set up the crossbeam on the base and be used for restricting the locating part of reaction vessel position each other, the locating part including set up in the spacing groove of one side on ground is kept away from at locating part both ends, the spacing groove with reaction vessel's tip agrees with under the condition of spacing groove with reaction vessel's first end block, reaction vessel does not use first end as the initial point with the second end of spacing groove block based on the power that transmission assembly transmitted, does circular motion in the vertical direction so that reaction vessel converts into upright gesture from the gesture of lying into gradually.

According to a preferred embodiment, the transmission assembly includes a power device, a first slider connected to and driven by the power device, a first sliding slot engaged with the first slider for guiding the first slider to move in a horizontal direction, a second sliding slot vertically connected to the first slider, a second slider engaged with the second sliding slot and guided by the second sliding slot to move in a direction perpendicular to the ground, and a transmission rod for connecting the second slider and the reaction vessel, wherein when the first slider moves in the guiding direction of the first sliding slot with the power device for many years, the second slider moves in the guiding direction of the second sliding slot under the action of a pulling force generated by the second slider by the transmission rod based on the gravity of the reaction vessel, and provides the pulling force to the reaction vessel to convert the reaction vessel from a lying posture to an upright posture.

According to a preferred embodiment, reaction vessel at least on first end and second end be provided with respectively a pair of can with the movable wheel of spacing groove block, the movable wheel with the locating part butt, and transmission's drive is in slide on the spacing distance between the spacing groove at both ends on the locating part, work as the movable wheel of second end with when the spacing groove block that corresponds with second end pulley on the locating part, the movable wheel of second end is used as the centre of a circle to reaction vessel's first end, uses reaction vessel's height to be the radius and does circular motion, so that reaction vessel converts into upright gesture from the gesture of lying into.

According to a preferred embodiment, the reaction vessel further comprises a degassing assembly, the degassing assembly at least comprises a degassing tube, a degassing pump and a degassing port, the degassing port is arranged on one side, far away from the ground, of the reaction vessel in the lying posture and is used for being connected with the degassing pump, one end, opposite to the degassing pump, of the degassing port is connected with the degassing tube, and when the reaction vessel is in the upright posture, the degassing tube is provided with a sealing assembly in a manner capable of preventing reaction substances from entering the degassing tube.

According to a preferred embodiment, the preparation apparatus further comprises a sterilization assembly including a jacket provided with a steam inlet, the jacket being disposed at a lower portion of the reaction vessel close to the ground when the reaction vessel is in an upright posture in such a manner as to form a receiving space for receiving steam with an outer wall of the reaction vessel, and the steam inlet of the jacket being disposed at an end of the jacket away from the ground in such a manner as to prevent backflow of condensed water when the reaction vessel is in an upright posture.

According to a preferred embodiment, the preparation device further comprises a control module, the control module is connected with the degassing assembly, the sterilization assembly and the transmission assembly, and when the degassing assembly is in the working state, the control module controls the transmission assembly to work so as to keep the reaction container in the lying state; when the sterilization assembly is in a working state, the control module controls the transmission assembly to work so as to keep the reaction container in an upright posture.

According to a preferred embodiment, the preparation device comprises a stirring shaft, wherein at least two stirring support shafts are arranged on the stirring shaft in a manner that the stirring performance of the preparation device can be increased, at least one stirring support shaft is provided with asymmetrically arranged stirring blades, and the stirring blades are provided with at least three through holes which are distributed in a disordered manner. When the preparation device is in a lying posture and the stirring shaft rotates, the stirring blade penetrates through liquid in the preparation device, and the liquid in contact with the stirring blade penetrates through the through hole under the action of pressure and gravity, so that turbulent flow is formed inside the preparation device.

According to a preferred embodiment, the preparation method comprises the following steps:

s1: the control module controls the temperature to be kept at 20-30 ℃, 30 parts of 4-methylbenzenesulfonic acid hydrazide, 30 parts of sodium bicarbonate, 8 parts of alumina, 12 parts of monosulfonate and 200 parts of distilled water are added into the reaction container, and the control module controls the transmission assembly to work so as to convert the reaction container (300) from an upright posture to a lying posture;

s2: the control module controls the stirring assembly to work so as to heat and stir the added substances for 3 hours;

s3: the control module controls the temperature of the reaction container to be reduced to 11-15 ℃, and controls the degassing component to work to degas the substances in the reaction container for 3-7 minutes;

s4: the control module controls the transmission assembly to work to convert the reaction vessel from the lying posture to the vertical posture, and controls the sterilization assembly to start working for sterilization for 15-20 minutes.

The invention has the beneficial technical effects that:

firstly, the synergist prepared from the components combines alkali and a surfactant, has high viscosity reduction rate, low cost and simple construction process, and is suitable for shallow, thin, thick and scattered heavy oil reservoirs.

Secondly, the synergist is prepared through a preparation device capable of changing between a lying posture and an upright posture, the preparation device adapts to different preparation processes through the change of the posture, and the area of a gas-liquid interface can be increased in the lying posture, so that the degassing speed is accelerated, and the preparation efficiency is improved.

Thirdly, the at least two stirring support shafts and the blades with the disordered through holes, which are arranged on the stirring support shafts in a staggered mode, can generate strong turbulence in the liquid in the preparation device through gravity and pressure, so that all reaction substances in the liquid can be mixed more fully, and the reaction efficiency and the product generation rate are improved.

Drawings

FIG. 1 is a front view of a preferred embodiment of a manufacturing apparatus of the present invention;

FIG. 2 is a side view of a preferred embodiment of a manufacturing apparatus of the present invention;

FIG. 3 is a schematic structural view of a preferred embodiment of the stirring assembly of the present invention.

List of reference numerals

100: the support assembly 200: the transmission assembly 300: reaction vessel

110: base 120: the cross beam 130: position limiting piece

131: the limiting groove 210: the power device 220: first chute

230: first slider 240: second runner 250: second slide block

260: the transmission rod 310: first end 320: second end

330: the movable wheel 340: left side 350: right side of the

360: feed inlet 370: the stirring component 371: electric machine

372: reducer 379: connecting rod 374: coupling device

375: stirring shaft 376: blade 377: stirring fulcrum shaft

378: and a through hole.

Detailed Description

The following detailed description is made with reference to the accompanying drawings.

Example 1

The invention provides a synergist, which comprises: 20-40 parts of 4-methylbenzene hydrazide, 20-40 parts of sodium bicarbonate, 5-10 parts of alumina, 10-15 parts of monosulfonate and 300 parts of distilled water.

Example 2

In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be considered as limiting the present invention.

The invention provides a preparation method of the synergist in example 1, which is to prepare the components of the synergist through a preparation device. The manufacturing apparatus shown in fig. 1 includes a reaction vessel 300, a support assembly 100, and a driving assembly 200. The reaction vessel 300 is connected to the support assembly 100 and the driving assembly 200, respectively, and when the reaction vessel 300 is in the lying posture, the support assembly 100 is located between the reaction vessel 300 and the ground, thereby functioning to support the reaction vessel 300. The transmission assembly 200 is disposed on the left side 340 or the right side 350 of the reaction vessel 300, so that force can be applied from the side to drive lying to switch between lying and standing postures, so as to adapt to different preparation processes and working conditions. Therefore, the efficiency of each preparation process is improved and the quality of the prepared synergist is improved by changing the posture of the preparation device.

According to a preferred embodiment, as shown in fig. 2, the support portion comprises: a base 110, a beam 120, and a limiting member 130. The base 110 is used for supporting the preparation device, enlarging the contact area of the preparation device and the bearing plane, thereby dispersing the pressure generated by the preparation device on the bearing plane and increasing the stability of the preparation device. At least two beams 120 are oppositely arranged on the base 110 at intervals, and an accommodating space is formed between the at least two beams 120. The accommodating space is used for accommodating the reaction vessel 300 in the lying posture. The height of the cross-beam 120 is determined according to the size of the reaction vessel 300. The reaction vessel 300 is preferably not in contact with the base 110 in the lying position. The stopper 130 serves to limit the position of the reaction vessel 300. At least two position-limiting members 130 intersect with the cross beam 120 and are disposed in parallel on a side of the cross beam 120 away from the base 110. The two ends of the limiting member 130 are respectively provided with a limiting groove 131. The two limiting grooves 131 are disposed on a side of the limiting member 130 away from the ground. The stopper grooves 131 can be engaged with both ends of the reaction vessel 300, so that the stopper 130 can restrict the movement space of the reaction vessel 300 between the stopper grooves 131. When the limiting groove 131 is partially engaged with the first end 310 of the reaction vessel 300, the second end 320 of the reaction vessel 300, which is not engaged with the limiting groove 131, performs a circular motion in a vertical plane based on the force transmitted by the transmission assembly 200 with the first end 310 as a center and the height of the reaction vessel 300 as a radius, and stops moving continuously when the reaction vessel 300 reaches an upright posture, thereby gradually converting the reaction vessel 300 from a lying posture to an upright posture.

Such a configuration is advantageous for adapting to different reaction processes in the reaction vessel 300, and increases factors that are advantageous for increasing the reaction rate in each reaction process through the change of the posture, thereby accelerating the reaction rate and improving the product quality. For example, when the synergist enters the degassing process and the stirring process, the reaction container 300 needs to be converted from the upright posture to the lying posture, and the lying posture can increase the contact surface area of the liquid and the air, so that the air in the liquid can be more quickly discharged out of the solution, and the degassing process is accelerated; when the stirring process is carried out, the stirring blade 376 of the stirring component 370 is in a vertical plane due to the lying posture of the preparation device, a part of liquid can be brought up in the stirring process, and the liquid falls down again due to gravity, so that the stirring effect is increased, the 4-methylbenzene sulfonyl hydrazide which is slightly soluble in water is fully mixed with the sodium hydroxide and the water, the solubility of the 4-methylbenzene sulfonyl hydrazide and other components in the synergist is increased, the components of the synergist are more uniform, and the using effect is more stable and reliable. When the synergist is in the sterilization or material-feeding process, the reaction container 300 needs to be changed from the lying posture to the upright posture to accelerate the material-feeding speed and improve the sterilization effect.

According to a preferred embodiment, as shown in fig. 1, the transmission assembly 200 comprises: a power device 210, a first slide block 230, a first slide slot 220, a second slide block 250, a second slide slot 240 and a transmission rod 260. The first sliding block 230 is connected with the power device 210 and then disposed in the first sliding slot 220, so that the power device 210 can move to drive the first sliding block 230 to move. The first sliding slot 220 is connected to the base 110 through a connecting plate, and is disposed on the left side 340 of the leftmost position 340 limiting member 130 or the right side 350 of the rightmost position 350 limiting member 130. The second sliding groove 240 is fixedly connected to the first sliding block 230, so that the movement of the first sliding block 230 can drive the second sliding groove 240 to move in the same direction. Preferably, after the second sliding chute 240 is connected to the first sliding block 230, the sliding chute direction of the second sliding chute 240 is perpendicular to the sliding direction of the first sliding chute 220. A second sliding block 250 engaged with the second sliding groove 240 is disposed in the second sliding groove 240. The second slider 250 is movable in the chute direction of the first chute 220. So that when the second chute 240 moves in the same direction as the first slide block 230 based on the power provided by the power unit 210 at the same time, the second slide block 250 can move in a direction perpendicular to the moving direction of the first slide block 230, thereby providing a sufficient variable amount to the reaction vessel 300 in the horizontal and vertical directions during posture change to ensure smooth switching of the reaction vessel 300 between the lying posture and the standing posture. The transmission rod 260 serves to connect the reaction vessel 300 and the second chute 240 so as to transmit the power of the transmission assembly 200 to the reaction vessel 300. One end of the transmission rod 260 is connected to the second sliding chute 240 through the second sliding block 250, so that when the second sliding block 250 moves along the guiding direction of the second sliding chute 240, the transmission rod 260 can be driven to move. The connection of the driving rod 260 with the reaction vessel 300 and the second slider 250 is a movable connection, preferably a rotary connection, to provide a sufficient displacement space for the posture change process of the reaction vessel 300. Preferably, when the driving assembly 200 is disposed at the leftmost side 340 of the reaction vessel 300, one end of the driving rod 260 opposite to the second slider 250 is connected to the leftmost side 340 of the cylindrical reaction vessel 300. When the driving assembly 200 is disposed at the rightmost side 350 of the reaction vessel 300, one end of the driving rod 260 opposite to the second slider 250 is coupled to the rightmost side 350 of the cylindrical reaction vessel 300. Therefore, when the reaction vessel 300 is driven by the transmission assembly 200 to be converted from the lying posture to the upright posture or from the upright posture to the lying posture, the motion trail of the reaction vessel 300 cannot be crossed with the motion trail of the transmission assembly 200 to cause the device to be stuck and unable to be used normally. With the above arrangement, power can be transmitted to the reaction container 300 by controlling the operating state of the power unit 210 in the transmission assembly 200, providing sufficient power and a movable space for the reaction container 300 to change the posture.

According to a preferred embodiment, as shown in FIG. 2, the reaction vessel 300 includes a first end 310 and a second end 320. The first end 310 is the end of the reaction vessel 300 that is farther from the ground when in the upright position, and the second end 320 is the end of the reaction vessel 300 that is closer to the ground when in the upright position. The reaction vessel 300 is provided with a pair of movable wheels 330 at least on the first end 310 and the second end 320, respectively. In the case where the reaction vessel 300 is in the lying posture, two pairs of movable wheels 330 respectively provided at the first end 310 and the second end 320 of the reaction vessel 300 are respectively provided at the left side 340 and the right side 350 of the reaction vessel 300 symmetrically in the horizontal direction. The movable wheel 330 can be engaged with the limiting grooves 131 at two ends of the limiting member 130, so as to be limited to move. The movable wheel 330 abuts against the limiting member 130, and the movable wheel 330 can move along the two limiting grooves 131 on the limiting member 130 under the driving of the power device 210. When the movable wheel 330330 of the first end 310 of the reaction container 300 is engaged with the corresponding limiting groove 131 of the limiting member 130, the second end 320 of the reaction container 300 is driven by the transmission assembly 200 to perform an arc motion with the movable wheel 330 of the first end 310 as a center and the height of the reaction container 300 as a radius, so that the reaction container 300 is converted from the lying posture to the upright posture. The arrangement mode enables the limiting part 130 to provide a fulcrum for the reaction container 300, so that the reaction container 300 can have a fixed circle center under the driving of the transmission assembly 200, thereby not only ensuring the posture change of the reaction container 300 under the driving of the transmission assembly 200, but also ensuring the stability of the reaction container 300 when the working posture is switched.

According to a preferred embodiment, the reaction vessel 300 further comprises a degassing assembly. The degasification subassembly includes: degassing port, degassing pipe, degassing valve and degassing pump. The degassing port is provided on the side of the reaction vessel 300 away from the ground when lying. The degassing pump is connected with the degassing port and used for providing power for a degassing process. One end of the degassing port opposite to the degassing pump is communicated with the inner cavity of the reaction vessel 300 through a degassing tube, so that gas in the liquid contained in the inner cavity of the reaction vessel 300 can be pumped out when the reaction vessel 300 is in the lying posture. The degassing tube is provided with a seal in such a manner that the reaction substance is prevented from entering the degassing tube when the reaction vessel 300 is in an upright posture. Preferably, the number of the degassing assemblies may be at least one, for example, two, three, four, etc., and the degassing pipes of the plurality of the degassing assemblies are respectively and uniformly arranged on one side of the reaction vessel 300 away from the ground in the lying posture, so that the suction force can be uniformly generated when the material degassing process is performed, the degassing speed is increased, and the material degassing is more sufficient.

According to a preferred embodiment, the reaction vessel 300 further comprises a sterilization assembly. The sterilization assembly includes a jacket provided with a steam inlet. The jacket is provided at the lower outer layer of the reaction vessel 300 and forms a hollow chamber for receiving steam with the outer layer of the vessel. In the case where the reaction vessel 300 is in the upright posture, the steam inlet of the jacket is provided at one end of the jacket away from the ground in such a manner that the reverse flow of the condensed water can be prevented. The jacket is provided to the reaction vessel 300 during the sterilization process, and high-temperature steam is introduced into the jacket through the steam inlet to heat the reaction vessel 300, thereby performing high-temperature sterilization on the reaction vessel 300. Such an arrangement is advantageous in that the material undergoing the degassing process can be sterilized immediately without being transferred to a sterilization apparatus for sterilization. The shock and contact with air during transport tend to re-entrain air into the already degassed synergist, thereby reducing the quality of the synergist. Therefore, the arrangement mode is tender, air can be prevented from being mixed into the synergist again, the time consumed by transportation is saved, the working process is accelerated, and the quality of the finished synergist is improved.

According to a preferred embodiment, the preparation device further comprises a control module, which is connected to the degassing assembly, the sterilization assembly and the transmission assembly 200 and is capable of controlling the operating state of each assembly individually. When entering the degassing process, the control module controls the transmission assembly 200 to keep the reaction vessel 300 in the lying posture and controls the degassing assembly to work to carry out degassing treatment on the synergist solution in the vessel. When entering the sterilization process, the control module controls the transmission assembly 200 to work so that the reaction container 300 keeps an upright posture, so that the heat of the steam introduced into the jacket can be quickly transferred to the synergist liquid in the sterilization process, the synergist liquid is fully sterilized, and the quality guarantee period and the use safety of the synergist are prolonged.

According to a preferred embodiment, the preparation device further comprises a temperature control assembly. The temperature control assembly comprises a coil and a thermometer. The arrangement of the coil and the thermometer is as in patent CN 209123900U.

According to a preferred embodiment, as shown in fig. 3, the preparation device further comprises a stirring assembly 370, wherein the stirring assembly 370 comprises a motor 371, a speed reducer 372, a coupler 374, a stirring shaft 375 and blades 376. The motor 371 is used to provide power. The motor 371 is connected with the speed reducer 372, and the speed reducer 372 is fixedly connected with the stirring shaft 375 through a coupling 374. The stirring assembly 370 is disposed along the central axis of the reaction vessel 300 at a time, the stirring shaft 375 and the blades 376 are disposed inside the reaction vessel 300, and the motor 371, the reducer 372, the conveyor belt and the coupling 374 are disposed outside the reaction vessel 300 and closely connected to the outer wall of the reaction vessel 300, so as to reduce the risk of liquid leakage and gas leakage. The blades 376 are fixedly connected with the stirring shaft 375 in a detachable manner, so that the stirring assembly 370 can be cleaned after use; and the single blade 376 assembly can be replaced when a problem occurs with the single blade 376 assembly to reduce waste of resources. When motor 371 is in operating condition, motor 371 can drive reduction gear 372 through the conveyer belt and function, and reduction gear 372 passes through shaft coupling 374 with power transmission for (mixing) shaft 375 and then drive (mixing) shaft 375 and rotate, and then drive and (mixing) shaft 375 fixed connection's stirring vane 376 rotates.

According to a preferred embodiment, the stirring shaft 375 is further provided with at least two stirring fulcrum 377. The stirring shaft 375 is connected to the stirring fulcrum 377 through a connecting rod 379. The connecting rod 379, the stirring shaft 375 and the stirring fulcrum 377 are integrally formed or fixedly connected. The fixed connection mode can be welding or bonding and the like. The stirring blades 376 are asymmetrically provided on at least one stirring fulcrum 377. At least three through holes 388 are arranged on the stirring blade 376 in a messy manner so as to increase the stirring effect. Preferably, the stirring blades 376 are asymmetrically arranged on the two stirring shafts 375. And, when the preparation facilities was in the gesture of lying, arbitrary two stirring vane 376 on two (mixing) shafts 375 were all not on same vertical line to make when (mixing) shaft 375 rotates, stirring fulcrum 377 and stirring vane 376 can make the inside liquid of reaction vessel produce strong turbulent flow, so that under gravity and stirring vane 376's effect, agitating unit's stirring effect is better, and the inside liquid reaction of reaction vessel is more abundant, and then promotes reaction rate and preparation efficiency.

According to a preferred embodiment, the reaction vessel 300 further comprises a feed inlet 360 and a discharge outlet. The feed inlet 360 is disposed at the second end 320 of the reaction vessel 300. The feed port 360 is provided at one side of the reaction vessel 300, which is far from the ground when lying in a posture, in a manner capable of reducing a risk of liquid leakage, and the feed port 360 is provided with a sealing member. The discharge port is arranged at the first end 310 of the reaction vessel 300 in a manner that can ensure the sterilization degree of the synergist, and the discharge port is arranged at the side of the reaction vessel 300 away from the ground when the reaction vessel is in the lying posture in a manner that can reduce the risk of leakage. The arrangement mode is favorable for discharging substances quickly, the substances cannot contact the part, which is not covered by the jacket, on the upper part of the reaction vessel 300 in the flowing process, the part is not sterilized thoroughly, and secondary pollution of the substances is easily caused, so that the arrangement mode of the discharge port can fully ensure the sterilization condition of the synergist.

Example 3

This example is a process for the preparation of the potentiator described in example 1, comprising the steps of:

s1: the control module controls the temperature control assembly to work so as to keep the temperature at 20-30 ℃; adding 30 parts of 4-methylbenzene sulfonyl hydrazide, 30 parts of sodium bicarbonate, 8 parts of aluminum oxide, 12 parts of monosulfonate and 200 parts of distilled water into a reaction container, and controlling a transmission assembly to work by a control module so as to convert the reaction container from a vertical posture to a lying state;

s2: the control module controls the stirring assembly to work so as to heat and stir the added substances for 3 hours;

s3: controlling the temperature control assembly to work to reduce the temperature of the reaction container to 11-15 ℃, and controlling the degassing assembly to work to degas the substances in the reaction container for 3-7 minutes;

s4: controlling the transmission assembly to work to convert the reaction vessel from the lying posture to the vertical posture, controlling the sterilization assembly to work, and sterilizing for 15-20 minutes.

It should be noted that the above-mentioned embodiments are exemplary, and that those skilled in the art, having benefit of the present disclosure, may devise various arrangements that are within the scope of the present disclosure and that fall within the scope of the invention. It should be understood by those skilled in the art that the present specification and figures are illustrative only and are not limiting upon the claims. The scope of the invention is defined by the claims and their equivalents.