1. A preparation method of a soft washing essence is characterized by comprising the following steps:

s1: preparing raw materials, namely 3-9 parts of ligustral, 2-8 parts of 2-pentylcyclopentanone, 2-10 parts of benzyl acetate, 3-7 parts of linalyl acetate, 10-30 parts of chrysanthemum essential oil, 3-15 parts of tulip ester, 12-24 parts of mint essential oil, 4-8 parts of lily essential oil, 3-6 parts of thickening agent, 5-12 parts of blending agent, 5-12 parts of emulsifier, 8-16 parts of fragrance fixing agent, 2-8 parts of modifier and 3-5 parts of benzyl alcohol;

s2: stirring and mixing, namely adding ligustral, 2-amyl cyclopentanone, benzyl acetate, linalyl acetate, chrysanthemum essential oil, tulip ester, mint essential oil, lily essential oil, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 50-90 minutes before preparation;

s3: adding blending agent, adding blending agent into mixing tank, mixing continuously, and heating while mixing;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fixative into a mixing tank, continuously stirring for 20-30 minutes, and then cooling;

s6: and (4) ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion to obtain a finished product.

2. The preparation method of the softening type washing essence according to claim 1, wherein the fixative in S5 is one or more of ambergris, musk, civet, castoreum, peru balsam, toluol, storax and oak moss extract.

3. The preparation method of a softening type washing essence according to claim 1, wherein the thickener in S2 is one or more of pectin, gelatin, gum arabic, agar, starch, sodium alginate, sodium caseinate and sodium carboxymethylcellulose.

4. The method of claim 1, wherein the fragrance combination of S3 is ilex pubescens essential oil prepared from ilex pubescens bark.

5. The preparation method of the softening type washing essence according to claim 1, wherein the ultrasonic dispersion time in the S6 is 15-25 minutes, and then the standing is performed for 10-20 minutes.

6. The preparation method of the softening type washing essence according to claim 3, wherein the emulsifier in S2 is one or more of glyceryl monostearate, soybean lecithin, sorbitan fatty acid ester and polyoxyethylene xylitol anhydride stearate.

7. The method for preparing a softening type washing essence according to claim 1, wherein the modifier in S4 is one or more of jasmine essential oil, orange essential oil, rose essential oil and vanilla essential oil, and the modifier is added and mixed, and then filtered by a 200-400 mesh sieve to remove impurities.

Background

The essence is a raw material for endowing cosmetics with certain fragrance, and is one of key raw materials in the manufacturing process. The essence is properly selected, is not only loved by consumers, but also can cover certain unpleasant odor in the product medium. The essence is prepared by blending and mixing a plurality of spices and has certain type of fragrance, namely aroma type, and when the cosmetics are perfumed, the proper aroma type is selected, and the selected essence has no influence on the product quality and the using effect.

Along with the improvement of living standard of people, detergents are updated, liquid detergents gradually replace original solid washing powder, detergent essence is promoted to be new, the odor of the detergent essence needs to be improved continuously, the existing detergent essence generally has the defects of insufficient smoothness, insufficient durability, no complete fermentation and single variety, and cannot meet the requirements of people.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides a preparation method of a softening type washing essence, and solves the problems that the existing washing essence generally has the defects of insufficient softening, insufficient durability, no hair penetration, single variety and incapability of meeting the requirements of people.

(II) technical scheme

In order to achieve the purpose, the invention provides the following technical scheme:

a preparation method of a soft washing essence comprises the following steps:

s1: preparing raw materials, namely 3-9 parts of ligustral, 2-8 parts of 2-pentylcyclopentanone, 2-10 parts of benzyl acetate, 3-7 parts of linalyl acetate, 10-30 parts of chrysanthemum essential oil, 3-15 parts of tulip ester, 12-24 parts of mint essential oil, 4-8 parts of lily essential oil, 3-6 parts of thickening agent, 5-12 parts of blending agent, 5-12 parts of emulsifier, 8-16 parts of fragrance fixing agent, 2-8 parts of modifier and 3-5 parts of benzyl alcohol;

s2: stirring and mixing, namely adding ligustral, 2-amyl cyclopentanone, benzyl acetate, linalyl acetate, chrysanthemum essential oil, tulip ester, mint essential oil, lily essential oil, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 50-90 minutes before preparation;

s3: adding blending agent, adding blending agent into mixing tank, mixing continuously, and heating while mixing;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fixative into a mixing tank, continuously stirring for 20-30 minutes, and then cooling;

s6: and (4) ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion to obtain a finished product.

As a further scheme of the invention, the fixative in S5 is one or more of ambergris, musk, civet, castoreum, peru balsam, Tulu balsam, benzoin resin, storax resin and oak moss extract.

Further, the thickener in S2 is one or more of pectin, gelatin, gum arabic, agar, starch, sodium alginate, sodium caseinate, and sodium carboxymethylcellulose.

Based on the scheme, the blending agent in the S3 is ilex latifolia essential oil which is prepared from the bark of ilex latifolia.

Further, the ultrasonic dispersion time in the S6 is 15-25 minutes, and then the standing is carried out for 10-20 minutes.

On the basis of the scheme, the emulsifier in the S2 is one or more of glyceryl monostearate, soybean lecithin, sorbitan fatty acid ester and polyoxyethylene xylitol anhydride stearate.

In a further scheme of the invention, the modifier in S4 is one or more of jasmine essential oil, orange essential oil, rose essential oil and vanilla essential oil, the modifier is added and mixed, and then the mixture is filtered by a sieve with 200 meshes and 400 meshes to remove impurities.

(III) advantageous effects

Compared with the prior art, the invention provides a preparation method of a soft and smooth washing essence, which has the following beneficial effects:

1. the compatible substances in the formula are green and healthy, the flowery odour of chrysanthemum, tulip, lily and the like is taken as the main part, and the spices of benzyl acetate, linalyl acetate and the like are used for modifying the fragrance to be smooth, wherein the 2-pentylcyclopentanone can ensure that the whole fragrance of the essence is more exquisite and full and the fragrance is more durable.

2. In the invention, the perfume fixative is not easy to volatilize, can inhibit the volatilization rate of other volatile perfumes, and can slow down the volatilization rate of the whole essence, and simultaneously can keep the fragrance characteristics or odor type of the essence consistent all the time so as to keep the essence with lasting fragrance.

3. According to the invention, the viscosity of the essence can be adjusted by adding the thickening agent, the emulsifying and stabilizing effects can be achieved by adding the emulsifying agent, and the thickening agent is matched to adjust the viscosity of the essence.

4. According to the invention, the addition of the modifier can adjust the style of the main fragrance according to different requirements, so that the diversity is improved, and the requirements of different people are met.

Drawings

Fig. 1 is a schematic flow structure diagram of a preparation method of a softening type washing essence provided by the invention.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

Referring to fig. 1, a preparation method of a softening type washing essence comprises the following steps:

s1: preparing raw materials, namely 4 parts of ligustral, 5 parts of 2-pentylcyclopentanone, 6 parts of benzyl acetate, 3 parts of linalyl acetate, 15 parts of chrysanthemum essential oil, 7 parts of tulip ester, 15 parts of mint essential oil, 5 parts of lily essential oil, 3 parts of thickening agent, 8 parts of fragrance blending agent, 6 parts of emulsifier, 9 parts of fragrance fixing agent, 3 parts of modifier and 3 parts of benzyl alcohol, wherein the fragrance of chrysanthemum, tulip, lily and the like is taken as a main part, and the fragrance of benzyl acetate, linalyl acetate and the like is modified to be round and more flexible, wherein the fragrance of the whole fragrance can be more exquisite and full through the use of 2-pentylcyclopentanone, and the fragrance can be more lasting;

s2: stirring and mixing, namely adding ligustral, 2-amyl cyclopentanone, benzyl acetate, linalyl acetate, chrysanthemum essential oil, tulip ester, mint essential oil, lily essential oil, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 65 minutes before preparation;

s3: adding blending agent, adding blending agent into mixing tank, mixing continuously, and heating while mixing;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fixative into a mixing tank, continuously stirring for 25 minutes, and then cooling;

s6: and (4) ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion to obtain a finished product.

The S5 fragrance fixative is ambergris and musk, through the addition of the fragrance fixative, the fragrance fixative is not easy to volatilize, the volatilization rate of other volatile spices can be inhibited, the volatilization rate of the whole essence is reduced, meanwhile, the fragrance characteristics or fragrance types of the essence can be kept consistent all the time, so that the essence with lasting fragrance is kept, the thickening agent in S2 is pectin and gelatin, the viscosity of the essence can be adjusted through the addition of the thickening agent, the fragrance fixative in S3 is ilex essential oil which is prepared from the bark of ilex, and the ilex essential oil has the functions of purging fire, detoxifying, clearing heat, promoting diuresis, promoting qi circulation, relieving pain, cooling blood and stopping bleeding, improves the diversity of the functions of the essence, and through the addition of the fragrance fixative, the fragrance of the main fragrance can be more harmonious and outstanding.

It is particularly noted that the ultrasonic dispersion time in the S6 is 18 minutes, then the ultrasonic dispersion time is 16 minutes, the emulsifier in the S2 is glyceryl monostearate, the emulsifying and stabilizing effect can be achieved through the addition of the emulsifier, the emulsifier is matched with a thickening agent to adjust the viscosity property of the essence, the modifiers in the S4 are jasmine essential oil, orange essential oil and rose essential oil, the modifiers are added and then mixed, then a 200-mesh sieve is used for filtering to remove impurities, the style of the main fragrance can be adjusted according to different requirements through the addition of the modifiers, and the diversity is improved, so that the requirements of different people are met.

Example 2

Referring to fig. 1, a preparation method of a softening type washing essence comprises the following steps:

s1: preparing raw materials, namely 4 parts of ligustral, 5 parts of 2-pentylcyclopentanone, 6 parts of benzyl acetate, 3 parts of linalyl acetate, 15 parts of chrysanthemum essential oil, 8 parts of tulip ester, 14 parts of mint essential oil, 5 parts of lily essential oil, 3 parts of thickening agent, 9 parts of blending agent, 5 parts of emulsifier, 9 parts of fragrance fixing agent, 3 parts of modifier and 3 parts of benzyl alcohol, wherein the fragrance of chrysanthemum, tulip, lily and the like is taken as a main part, and the fragrance of benzyl acetate, linalyl acetate and the like is modified to be round and more smooth, wherein the fragrance is more delicate and full due to the use of 2-pentylcyclopentanone, and the fragrance is more lasting;

s2: stirring and mixing, namely adding ligustral, 2-amyl cyclopentanone, benzyl acetate, linalyl acetate, chrysanthemum essential oil, tulip ester, mint essential oil, lily essential oil, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 75 minutes before preparation;

s3: adding blending agent, adding blending agent into mixing tank, mixing continuously, and heating while mixing;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fixative into a mixing tank, continuously stirring for 28 minutes, and then cooling;

s6: and (4) ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion to obtain a finished product.

The fragrance fixing agent in the S5 is castoreum, Peru balsam, Tulu balsam, benzoin resin, storax resin and oak moss extract, the fragrance fixing agent is not easy to volatilize, the volatilization rate of other volatile spices can be inhibited, the volatilization rate of the whole essence is reduced, the fragrance characteristics or fragrance types of the essence can be kept consistent all the time to keep the fragrance lasting, the thickening agent in the S2 is one or more of sodium caseinate and sodium carboxymethylcellulose, the viscosity of the essence can be adjusted by adding the thickening agent, the fragrance fixing agent in the S3 is ilex essential oil which is prepared from the bark of ilex latifolia L, and the ilex latifolia L has the functions of purging fire, detoxifying, clearing heat, promoting diuresis, promoting qi circulation, relieving pain, cooling blood and stopping bleeding, and the diversity of the functions of the essence can make the fragrance of the main fragrance agent more coordinated and prominent.

Particularly, the ultrasonic dispersion time in S6 is 20 minutes, then the ultrasonic dispersion time is 16 minutes, the emulsifier in S2 is glyceryl monostearate and soybean lecithin, the emulsifying stabilization effect can be achieved through the addition of the emulsifier, the emulsifier is matched with a thickening agent to adjust the viscosity property of essence, the modifier in S4 is one or more of jasmine essential oil, orange essential oil, rose essential oil and vanilla essential oil, the modifier is added and then mixed, then the mixture is filtered by a 200-mesh sieve to remove impurities, the style of main fragrance can be adjusted according to different requirements through the addition of the modifier, the diversity is improved, and therefore the requirements of different people are met.

Example 3

Referring to fig. 1, a preparation method of a softening type washing essence comprises the following steps:

s1: preparing raw materials, namely 6 parts of ligustral, 5 parts of 2-pentylcyclopentanone, 5 parts of benzyl acetate, 3 parts of linalyl acetate, 15 parts of chrysanthemum essential oil, 7 parts of tulip ester, 15 parts of mint essential oil, 5 parts of lily essential oil, 3 parts of thickening agent, 10 parts of fragrance blending agent, 6 parts of emulsifier, 7 parts of fragrance fixing agent, 3 parts of modifier and 3 parts of benzyl alcohol, wherein the fragrance of chrysanthemum, tulip, lily and the like is taken as a main part, and the fragrance of benzyl acetate, linalyl acetate and the like is modified to be round and more flexible, wherein the fragrance of the whole fragrance can be more exquisite and full through the use of 2-pentylcyclopentanone, and the fragrance can be more lasting;

s2: stirring and mixing, namely adding ligustral, 2-amyl cyclopentanone, benzyl acetate, linalyl acetate, chrysanthemum essential oil, tulip ester, mint essential oil, lily essential oil, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 65 minutes before preparation;

s3: adding blending agent, adding blending agent into mixing tank, mixing continuously, and heating while mixing;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fixative into a mixing tank, continuously stirring for 25 minutes, and then cooling;

s6: and (4) ultrasonic dispersion, namely putting the stirred mixture into an ultrasonic dispersion machine for ultrasonic dispersion to obtain a finished product.

The fragrance fixative in S5 is Peru balsam resin, through the addition of the fragrance fixative, the fragrance fixative is not easy to volatilize, but also can inhibit the volatilization rate of other volatile spices, so that the volatilization rate of the whole essence is slowed down, and simultaneously the fragrance characteristics or odor types of the essence can be kept consistent all the time so as to keep the essence with lasting fragrance, the thickening agent in S2 is starch, the viscosity of the essence can be adjusted through the addition of the thickening agent, the fragrance fixative in S3 is ilex essential oil which is prepared from the bark of ilex, and the essence has the functions of purging fire, detoxifying, clearing heat, promoting diuresis, promoting qi circulation, relieving pain, cooling blood and stopping bleeding, and improves the diversity of the functions of the essence, and the addition of the fragrance fixative can enable the fragrance of the main fragrance to be more coordinated and prominent.

The ultrasonic dispersion time in S6 is 18 minutes, then the ultrasonic dispersion time is 16 minutes, the emulsifier in S2 is sorbitan fatty acid ester, the emulsifying stabilization effect can be achieved through the addition of the emulsifier, the thickener is matched to adjust the viscosity performance of the essence, the modifier in S4 is jasmine essential oil and orange essential oil, the jasmine essential oil and the orange essential oil are mixed after the modifier is added, then a 200-mesh sieve is used for filtering, impurities are removed, the style of the main fragrance can be adjusted according to different requirements through the addition of the modifier, the diversity is improved, and therefore the requirements of different people are met.

In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.